ASTM E314 - 10(2015)e1

    Standard Test Methods for Determination of Manganese in Iron Ores by Pyrophosphate (Potentiometric) and Periodate (Spectrophotometric) Techniques

    Active Standard ASTM E314 | Developed by Subcommittee: E01.02

    Book of Standards Volume: 03.05


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    Significance and Use

    4.1 This test method is intended to be used for compliance with compositional specifications for manganese content in iron ores, concentrates, and agglomerates. It is assumed that all who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E882.

    1. Scope

    1.1 These test methods cover the determination of manganese in iron ores, concentrates, and agglomerates. The following two test methods are included:

     

    Sections

     Test Method A (Pyrophosphate (Potentiometric))

    8 – 15

     Test Method B (Periodate (Photometric))

    16 – 22

    1.2 Test Method A covers the determination of manganese in the range from 2.5 % to 15.0 %. Test Method  B covers the determination of manganese in the range of 0.01 % to 5.00 %.

    Note 1: The lower limit for this test method is set at 50 % relative error for the lowest grade material tested in the interlaboratory study in accordance with Practice E1601.

    1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

    E135 Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials

    E173 Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals

    E877 Practice for Sampling and Sample Preparation of Iron Ores and Related Materials for Determination of Chemical Composition

    E882 Guide for Accountability and Quality Control in the Chemical Analysis Laboratory

    E1601 Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method


    ICS Code

    ICS Number Code 73.060.10 (Iron ores)

    UNSPSC Code

    UNSPSC Code 11101601(Iron ore)


    Referencing This Standard
    Link Here
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    DOI: 10.1520/E0314-10R15E01

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    Citation Format

    ASTM E314-10(2015)e1, Standard Test Methods for Determination of Manganese in Iron Ores by Pyrophosphate (Potentiometric) and Periodate (Spectrophotometric) Techniques, ASTM International, West Conshohocken, PA, 2015, www.astm.org

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