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Significance and Use
4.1 These practices are primarily intended to test materials for compliance with compositional specifications and for monitoring. Partial extraction of ores and related metallurgical materials can provide information on the availability of elements to leaching, water quality changes, or other site conditions.
4.2 It is assumed that the users of these practices will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices such as those described in Guide shall be followed.
1.1 These practices cover the digestion of ores and related metallurgical materials, such as mine soil, waste rock and tailings, for subsequent determination of acid-extractable contents of certain elements by such solution analytical techniques as atomic absorption spectrometry (AAS), atomic emission spectrometry (ICP-AES), (see Test Method ), and inductively coupled plasma mass spectrometry (ICP-MS) (see Test Method ).
1.1.1 Contents of aluminum, antimony, arsenic, barium, beryllium, bismuth, boron, cadmium, calcium, chromium, cobalt, copper, gallium, iron, lead, lithium, magnesium, manganese, mercury, molybdenum, nickel, phosphorus, potassium, scandium, selenium, silver, sodium, strontium, thallium, tin, titanium, vanadium and zinc can be extracted from ores and related metallurgical materials for determination by analytical methods for elements in solution. Other elements may be determined from extracts produced using this practice.
1.1.2 Actual element quantification in digested solutions can be accomplished by following the various test methods under other appropriate ASTM standards for element(s) of interest in solution.
1.1.3 The detection limit and linear content range for each element is dependent on the atomic absorption, mass spectrometry or emission spectrometric technique employed and may be found in the manual accompanying the instrument used or ASTM standard method for analysis of the solutions. Take into account the dilution factor in content calculations due to digestion and dilution of solid samples.
1.1.4 The extent of extraction of elements from ores and related metallurgical materials by these practices is dependent upon the physical and mineralogical characteristics of the prepared sample and the digestion practice used.
1.2 The digestion practices appear in the following order:
Nitric Acid Microwave Digestion
Four-Acid Total Digestion
1.3 The values stated SI units are to be regarded as the standard. No other units of measurements are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section .
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D1193 Specification for Reagent Water
D1976 Test Method for Elements in Water by Inductively-Coupled Argon Plasma Atomic Emission Spectroscopy
D5258 Practice for Acid-Extraction of Elements from Sediments Using Closed Vessel Microwave Heating
D5673 Test Method for Elements in Water by Inductively Coupled Plasma--Mass Spectrometry
E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
E135 Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
E882 Guide for Accountability and Quality Control in the Chemical Analysis Laboratory
Federal StandardCFRTitle21, Part 1030, and Title 47, Part 18
ICS Number Code 73.060.01 (Metalliferrous minerals and their concentrates in general)
UNSPSC Code 11101600(Ores)
ASTM E2941-14, Standard Practices for Extraction of Elements from Ores and Related Metallurgical Materials by Acid Digestion, ASTM International, West Conshohocken, PA, 2014, www.astm.orgBack to Top