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ASTM E2338-22

Standard Practice for Characterization of Coatings Using Conformable Eddy Current Sensors without Coating Reference Standards

Standard Practice for Characterization of Coatings Using Conformable Eddy Current Sensors without Coating Reference Standards E2338-22 ASTM|E2338-22|en-US Standard Practice for Characterization of Coatings Using Conformable Eddy Current Sensors without Coating Reference Standards Standard new BOS Vol. 03.03 Committee E07
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Significance and Use

4.1 Conformable Eddy Current Sensors—Conformable, eddy current sensors can be used on both flat and curved surfaces, including fillets, cylindrical surfaces, etc. When used with models for predicting the sensor response and appropriate algorithms, these sensors can measure variations in physical properties, such as electrical conductivity or magnetic permeability, or both, as well as thickness of conductive coatings on any substrate and nonconductive coatings on conductive substrates or on a conducting coating. These property variations can be used to detect and characterize heterogeneous regions within the conductive coatings, for example, regions of locally higher porosity.

4.2 Sensors and Sensor Arrays—Depending on the application, either a single-sensing element sensor or a sensor array can be used for coating characterization. A sensor array provides a better capability to map spatial variations in coating thickness or conductivity, or both (reflecting, for example, porosity variations), and provides better throughput for scanning large areas. The size of the sensor footprint and the size and number of sensing elements within an array depend on the application requirements and constraints, and the nonconductive (for example, ceramic) coating thickness.

4.3 Coating Thickness Range—The conductive coating thickness range over which a sensor performs best depends on the difference between the electrical conductivity of the substrate and conductive coating and available frequency range. For example, a specific sensor geometry with a specific frequency range for impedance measurements may provide acceptable performance for an MCrAlY coating over a nickel-alloy substrate for a relatively wide range of conductive coating thickness, for example, from 75 to 400 μm (0.003 to 0.016 in.). Yet, for another conductive coating-substrate combination, this range may be 10 to 100 μm (0.0004 to 0.004 in.). The coating characterization performance may also depend on the thickness of a nonconductive topcoat. For any coating system, performance verification on representative coated specimens is critical to establishing the range of optimum performance. For nonconductive coatings, such as ceramic coatings, the thickness measurement range increases with an increase of the spatial wavelength of the sensor (for example, thicker coatings can be measured with larger sensor winding spatial wavelength). For nonconductive coatings, when roughness of the coating may have a significant effect on the thickness measurement, independent measurements of the nonconductive coating roughness, for example, by profilometry, may provide a correction for the roughness effects.

4.4 Process-Affected Zone—For some processes, for example, shot peening, the process-affected zone can be represented by an effective layer thickness and conductivity. These values can in turn be used to assess process quality. A strong correlation must be demonstrated between these “effective coating” properties and process quality.

4.5 Three-Unknown Algorithm—Use of multiple-frequency impedance measurements and a three-unknown algorithm permits independent determination of three unknowns: (1) thickness of conductive nonmagnetic coatings, (2) conductivity of conductive nonmagnetic coatings, and (3) lift-off that provides a measure of the nonconductive coating thickness.

4.6 Accuracy—Depending on the material properties and frequency range, there is an optimal measurement performance range for each coating system. The instrument, its air standardization or reference substrate standardization, or both, and its operation permit the coating thickness to be determined within ±15 % of its true thickness for coating thickness within the optimal range and within ±30 % outside the optimal range. Better performance may be required for some applications.

4.7 Databases for Sensor Response—Databases of sensor responses may be used to represent the model response for the sensor. These databases may be based upon physical models or empirical relations. The databases list expected sensor responses (for example, the real and imaginary parts or the magnitude and phase of the complex transimpedance between the sense element and drive winding) over relevant ranges in the properties of interest. Example properties for a coated substrate material are the magnetic permeability or electrical conductivity of the substrate, or both, the electrical conductivity and thickness of the coating, and the lift-off. The ranges of the property values within the databases should span the expected property ranges for the material system to be examined.

Scope

1.1 This practice covers the use of conformable eddy current sensors for nondestructive characterization of coatings without standardization on coated reference parts. It includes the following: (1) thickness measurement of a conductive coating on a conductive substrate, (2) detection and characterization of local regions of increased porosity of a conductive coating, and (3) measurement of thickness for nonconductive coatings on a conductive substrate or on a conductive coating. This practice includes only nonmagnetic coatings on either magnetic (μ ≠ μ0) or nonmagnetic (μ = μ0) substrates. In addition to discrete coatings on substrates, this practice can also be used to measure the effective thickness of a process-affected zone (for example, shot peened layer for aluminum alloys, alpha case for titanium alloys) and to assess the condition of other layered media such as joints (for example, lap joints and skin panels over structural supports). For specific types of coated parts, the user may need a more specific procedure tailored to a specific application.

1.2 Specific uses of conventional eddy current sensors are covered by Practices D7091 and E376 and the following test methods issued by ASTM: B244 and E1004. Guidance for the use of conformable eddy current sensor arrays is provided in Guide E2884.

1.3 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Details
Book of Standards Volume: 03.03
Developed by Subcommittee: E07.07
Pages: 9
DOI: 10.1520/E2338-22
ICS Code: 25.220.01