ASTM E1921 - 13a

    Standard Test Method for Determination of Reference Temperature, To, for Ferritic Steels in the Transition Range

    Active Standard ASTM E1921 | Developed by Subcommittee: E08.07

    Book of Standards Volume: 03.01

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    Significance and Use

    5.1 Fracture toughness is expressed in terms of an elastic-plastic stress intensity factor, KJc, that is derived from the J-integral calculated at fracture.

    5.2 Ferritic steels are inhomogeneous with respect to the orientation of individual grains. Also, grain boundaries have properties distinct from those of the grains. Both contain carbides or nonmetallic inclusions that can act as nucleation sites for cleavage microcracks. The random location of such nucleation sites with respect to the position of the crack front manifests itself as variability of the associated fracture toughness (13). This results in a distribution of fracture toughness values that is amenable to characterization using statistical methods.

    5.3 Distributions of KJc data from replicate tests can be used to predict distributions of KJc for different specimen sizes. Theoretical reasoning (9), confirmed by experimental data, suggests that a fixed Weibull slope of 4 applies to all data distributions and, as a consequence, standard deviation on data scatter can be calculated. Data distribution and specimen size effects are characterized using a Weibull function that is coupled with weakest-link statistics (14). An upper limit on constraint loss and a lower limit on test temperature are defined between which weakest-link statistics can be used.

    5.4 The experimental results can be used to define a master curve that describes the shape and location of median KJc transition temperature fracture toughness for 1T specimens (15). The curve is positioned on the abscissa (temperature coordinate) by an experimentally determined reference temperature, To. Shifts in reference temperature are a measure of transition temperature change caused, for example, by metallurgical damage mechanisms.

    5.5 Tolerance bounds on KJc can be calculated based on theory and generic data. For added conservatism, an offset can be added to tolerance bounds to cover the uncertainty associated with estimating the reference temperature, To, from a relatively small data set. From this it is possible to apply a margin adjustment to To in the form of a reference temperature shift.

    5.6 For some materials, particularly those with low strain hardening, the value of To may be influenced by specimen size due to a partial loss of crack-tip constraint (5). When this occurs, the value of To may be lower than the value that would be obtained from a data set of KJc values derived using larger specimens.

    5.7 As discussed in 1.3, there is an expected bias among To values as a function of the standard specimen type. The magnitude of the bias may increase inversely to the strain hardening ability of the test material at a given yield strength, as the average crack-tip constraint of the data set decreases (16). On average, To values obtained from C(T) specimens are higher than To values obtained from SE(B) specimens. Best estimate comparison indicates that the average difference between C(T) and SE(B)-derived To values is approximately 10 °C (2). However, individual C(T) and SE(B) datasets may show much larger To differences (3, 17, 18), or the SE(B) To values may be higher than the C(T) values (2) . On the other hand, comparisons of individual, small datasets may not necessarily reveal this average trend. Datasets which contain both C(T) and SE(B) specimens may generate To results which fall between the To values calculated using solely C(T) or SE(B) specimens.

    1. Scope

    1.1 This test method covers the determination of a reference temperature, To, which characterizes the fracture toughness of ferritic steels that experience onset of cleavage cracking at elastic, or elastic-plastic KJc instabilities, or both. The specific types of ferritic steels (3.2.1) covered are those with yield strengths ranging from 275 to 825 MPa (40 to 120 ksi) and weld metals, after stress-relief annealing, that have 10 % or less strength mismatch relative to that of the base metal.

    1.2 The specimens covered are fatigue precracked single-edge notched bend bars, SE(B), and standard or disk-shaped compact tension specimens, C(T) or DC(T). A range of specimen sizes with proportional dimensions is recommended. The dimension on which the proportionality is based is specimen thickness.

    1.3 Median KJc values tend to vary with the specimen type at a given test temperature, presumably due to constraint differences among the allowable test specimens in 1.2. The degree of K Jc variability among specimen types is analytically predicted to be a function of the material flow properties (1)2 and decreases with increasing strain hardening capacity for a given yield strength material. This KJc dependency ultimately leads to discrepancies in calculated T o values as a function of specimen type for the same material. To values obtained from C(T) specimens are expected to be higher than T o values obtained from SE(B) specimens. Best estimate comparisons of several materials indicate that the average difference between C(T) and SE(B)-derived To values is approximately 10°C (2). C(T) and SE(B) To differences up to 15°C have also been recorded (3). However, comparisons of individual, small datasets may not necessarily reveal this average trend. Datasets which contain both C(T) and SE(B) specimens may generate To results which fall between the To values calculated using solely C(T) or SE(B) specimens. It is therefore strongly recommended that the specimen type be reported along with the derived T o value in all reporting, analysis, and discussion of results. This recommended reporting is in addition to the requirements in 11.1.1.

    1.4 Requirements are set on specimen size and the number of replicate tests that are needed to establish acceptable characterization of KJc data populations.

    1.5 To is dependent on loading rate. T o is evaluated for a quasi-static loading rate range with 0.1< dK/dt < 2 MPa√m/s. Slowly loaded specimens (dK/dt < 0.1 MPa√m) can be analyzed if environmental effects are known to be negligible. Provision is also made for higher loading rates (dK/dt > 2 MPa√m/s).

    1.6 The statistical effects of specimen size on KJc in the transition range are treated using weakest-link theory (4) applied to a three-parameter Weibull distribution of fracture toughness values. A limit on KJc values, relative to the specimen size, is specified to ensure high constraint conditions along the crack front at fracture. For some materials, particularly those with low strain hardening, this limit may not be sufficient to ensure that a single-parameter (K Jc) adequately describes the crack-front deformation state (5).

    1.7 Statistical methods are employed to predict the transition toughness curve and specified tolerance bounds for 1T specimens of the material tested. The standard deviation of the data distribution is a function of Weibull slope and median KJc. The procedure for applying this information to the establishment of transition temperature shift determinations and the establishment of tolerance limits is prescribed.

    1.8 The fracture toughness evaluation of nonuniform material is not amenable to the statistical analysis methods employed in this standard. Materials must have macroscopically uniform tensile and toughness properties. For example, multipass weldments can create heat-affected and brittle zones with localized properties that are quite different from either the bulk material or weld. Thick section steel also often exhibits some variation in properties near the surfaces. Metallography and initial screening may be necessary to verify the applicability of these and similarly graded materials. Particular notice should be given to the 2% and 98% tolerance bounds on KJc presented in 9.3. Data falling outside these bounds may indicate nonuniform material properties.

    1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    E4 Practices for Force Verification of Testing Machines

    E8/E8M Test Methods for Tension Testing of Metallic Materials

    E23 Test Methods for Notched Bar Impact Testing of Metallic Materials

    E74 Practice of Calibration of Force-Measuring Instruments for Verifying the Force Indication of Testing Machines

    E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods

    E208 Test Method for Conducting Drop-Weight Test to Determine Nil-Ductility Transition Temperature of Ferritic Steels

    E399 Test Method for Linear-Elastic Plane-Strain Fracture Toughness KIc of Metallic Materials

    E436 Test Method for Drop-Weight Tear Tests of Ferritic Steels

    E561 Test Method for K-R Curve Determination

    E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

    E1820 Test Method for Measurement of Fracture Toughness

    E1823 Terminology Relating to Fatigue and Fracture Testing

    ICS Code

    ICS Number Code 77.040.10 (Mechanical testing of metals)

    UNSPSC Code

    UNSPSC Code 41000000(Laboratory and Measuring and Observing and Testing Equipment)

    DOI: 10.1520/E1921

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