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Significance and Use
5.1 This test method has advantages in certain respects over the use of static loading systems for measuring moduli.
5.1.1 This test method is nondestructive in nature. Only minute stresses are applied to the specimen, thus minimizing the possibility of fracture.
5.1.2 The period of time during which measurement stress is applied and removed is of the order of hundreds of microseconds. With this test method it is feasible to perform measurements at high temperatures, where delayed elastic and creep effects would invalidate modulus of elasticity measurements calculated from static loading.
5.2 This test method is suitable for detecting whether a material meets the specifications, if cognizance is given to one important fact in materials are often sensitive to thermal history. Therefore, the thermal history of a test specimen must be considered in comparing experimental values of moduli to reference or standard values. Specimen descriptions should include any specific thermal treatments that the specimens have received.
1.1 This test method covers the determination of the dynamic elastic properties of elastic materials. Specimens of these materials possess specific mechanical resonant frequencies that are determined by the modulus of elasticity, mass, and geometry of the test specimen. Therefore, the dynamic elastic properties of a material can be computed if the geometry, mass, and mechanical resonant frequencies of a suitable test specimen of that material can be measured. Dynamic Young's modulus is determined using the resonant frequency in the flexural mode of vibration. The dynamic shear modulus, or modulus of rigidity, is found using torsional resonant vibrations. Dynamic Young's modulus and dynamic shear modulus are used to compute Poisson's ratio.
1.2 This test method is specifically appropriate for materials that are elastic, homogeneous, and isotropic (1).2 Materials of a composite character (particulate, whisker, or fiber reinforced) may be tested by this test method with the understanding that the character (volume fraction, size, morphology, distribution, orientation, elastic properties, and interfacial bonding) of the reinforcement in the test specimen will have a direct effect on the elastic properties. These reinforcement effects must be considered in interpreting the test results for composites. This test method is not satisfactory for specimens that have cracks or voids that are major discontinuities in the specimen. Neither is the test method satisfactory when these materials cannot be fabricated in a uniform rectangular or circular cross section.
1.3 A high-temperature furnace and cryogenic cabinet are described for measuring the dynamic elastic moduli as a function of temperature from –195 to 1200°C.
1.4 Modification of this test method for use in quality control is possible. A range of acceptable resonant frequencies is determined for a specimen with a particular geometry and mass. Any specimen with a frequency response falling outside this frequency range is rejected. The actual modulus of each specimen need not be determined as long as the limits of the selected frequency range are known to include the resonant frequency that the specimen must possess if its geometry and mass are within specified tolerances.
1.5 There are material-specific ASTM standards that cover the determination of resonance frequencies and elastic properties of specific materials by sonic resonance or by impulse excitation of vibration. Test Methods C215, C623, C747, C848, C1198, and C1259 may differ from this test method in several areas (for example; sample size, dimensional tolerances, sample preparation). The testing of these materials shall be done in compliance with these material specific standards. Where possible, the procedures, sample specifications, and calculations are consistent with these test methods.
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
C215 Test Method for Fundamental Transverse, Longitudinal, and Torsional Resonant Frequencies of Concrete Specimens
C623 Test Method for Youngs Modulus, Shear Modulus, and Poissons Ratio for Glass and Glass-Ceramics by Resonance
C747 Test Method for Moduli of Elasticity and Fundamental Frequencies of Carbon and Graphite Materials by Sonic Resonance
C848 Test Method for Youngs Modulus, Shear Modulus, and Poissons Ratio For Ceramic Whitewares by Resonance
C1198 Test Method for Dynamic Youngs Modulus, Shear Modulus, and Poissons Ratio for Advanced Ceramics by Sonic Resonance
C1259 Test Method for Dynamic Youngs Modulus, Shear Modulus, and Poissons Ratio for Advanced Ceramics by Impulse Excitation of Vibration
E6 Terminology Relating to Methods of Mechanical Testing
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ICS Number Code 81.060.20 (Ceramic products)