Active Standard ASTM D7771 | Developed by Subcommittee: D24.66
Book of Standards Volume: 09.01
Historical (view previous versions of standard)
Significance and Use
5.1 This test procedure is used to determine the concentration of BaP extracted from carbon black by the means of a Soxhlet extraction apparatus with toluene.
1.1 This test method covers the qualitative and quantitative determination of only benzo-α-pyrene (BaP), a specific polycyclic aromatic hydrocarbon (PAH), on carbon black. The procedure involves Soxhlet extraction with toluene and analysis by gas chromatography with mass spectrometry (GC/MS). This method is not intended to test for U.S. Food and Drug Administration (FDA 21 CFR 178.3297) compliance of carbon blacks used for indirect food contact applications.
1.2 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D4483 Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
EPA StandardMethod8270D Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Federal Standard21CFR178.3297 Indirect Food Additives: Adjuvants, Productions Aids, and Sanitizers, Colorants for Polymers Available from the U.S. Government Printing Office, Superintendent of Documents, 732 N. Capital St., NW., Washington, DC 20402-0001.
ICS Number Code 83.040.20 (Rubber compounding ingredients)