ASTM D7419 - 13

    Standard Test Method for Determination of Total Aromatics and Total Saturates in Lube Basestocks by High Performance Liquid Chromatography (HPLC) with Refractive Index Detection

    Active Standard ASTM D7419 | Developed by Subcommittee: D02.04.0C

    Book of Standards Volume: 05.04

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    Significance and Use

    5.1 The composition of a lubricating oil has a large effect on the characteristics and uses of the oil. The determination of saturates, aromatics and polars is a key analysis of this composition. The characterization of the composition of lubricating oils is important in determining their interchangeability for use in blending etcetera.

    1. Scope

    1.1 This test method covers the determination of total aromatics and total saturates in additive-free lube basestocks using high performance liquid chromatography (HPLC) with refractive index (RI) detection. This test method is applicable to samples containing total aromatics in the concentration range of 0.2 to 46 mass %.

    1.1.1 Polar compounds, if present, are combined with the total aromatics. Precision was determined for basestocks with polars content < 1.0 mass %.

    1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D4057 Practice for Manual Sampling of Petroleum and Petroleum Products

    D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products

    D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance

    ICS Code

    ICS Number Code 75.100 (Lubricants, industrial oils and related products)

    UNSPSC Code

    UNSPSC Code 15101500(Petroleum and distillates)

    DOI: 10.1520/D7419

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