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Significance and Use
5.1 This procedure describes a rapid and sensitive method for estimating the stability reserve of an oil. The stability reserve is estimated in terms of a separability number, where a low value of the separability number indicates that there is a stability reserve within the oil. When the separability number is between 0 to 5, the oil can be considered to have a high stability reserve and asphaltenes are not likely to flocculate. If the separability number is between 5 to 10, the stability reserve in the oil will be much lower. However, asphaltenes are, in this case, not likely to flocculate as long as the oil is not exposed to any worse conditions, such as storing, aging, and heating. If the separability number is above 10, the stability reserve of the oil is very low and asphaltenes will easily flocculate, or have already started to flocculate.
5.2 This test method can be used by refiners and users of oils, for which this test method is applicable, to estimate the stability reserves of their oils. Hence, this test method can be used by refineries to control and optimize their refinery processes. Consumers of oils can use this test method to estimate the stability reserve of their oils before, during, and after storage.
5.3 This test method is not intended for predicting whether oils are compatible before mixing, but can be used for determining the separability number of already blended oils. However, oils that show a low separability number are more likely to be compatible with other oils than are oils with high separability numbers.
1.1 This test method covers the quantitative measurement, either in the laboratory or in the field, of how easily asphaltene-containing heavy fuel oils diluted in toluene phase separate upon addition of heptane. This is measured as a separability number (%) by the use of an optical scanning device.
1.2 The test method is limited to asphaltene-containing heavy fuel oils. ASTM specification fuels that generally fall within the scope of this test method are Specification D396, Grade Nos. 4, 5, and 6, Specification D975, Grade No. 4-D, and Specification D2880, Grade Nos. 3-GT and 4-GT. Refinery fractions from which such blended fuels are made also fall within the scope of this test method.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D396 Specification for Fuel Oils
D975 Specification for Diesel Fuel Oils
D2880 Specification for Gas Turbine Fuel Oils
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
ICS Number Code 71.080.10 (Aliphatic hydrocarbons)
UNSPSC Code 15101702(#4 or #6 Residual heavy fuel oils)
ASTM D7061-12, Standard Test Method for Measuring n-Heptane Induced Phase Separation of Asphaltene-Containing Heavy Fuel Oils as Separability Number by an Optical Scanning Device, ASTM International, West Conshohocken, PA, 2012, www.astm.orgBack to Top