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Significance and Use
5.1 These guidelines provide procedures for manually collecting gross samples from beneath the exposed surface of coal in railroad cars, barges, trucks, or stockpiles taking into account the wide variety of conditions that may be encountered. The samples are further processed for the laboratory to provide estimations of the coal quality. The use of this practice is conditional upon agreement among all interested parties concerning all relevant details of sample collection before sampling begins. These include, but are not limited to: lot size; number and mass of increments; the size, shape, and manipulation of the increment collection devices; location of increment collection site or sites; circumstances under which increments are not to be collected or suspended; and safety precautions. It is preferable that such agreements be in writing. The user is cautioned that samples so obtained do not represent material below the point of penetration.
1.1 This practice covers procedures for obtaining a manual gross sample from beneath the surface of coal in railroad cars, barges, trucks, or stockpiles. These procedures are to be used to provide gross samples for estimating the quality of the coal. The gross samples are to be crushed, divided, and further prepared for analysis in accordance with Practice D2013.
1.2 This practice provides instruction for sampling beneath the exposed surface coal to a depth of approximately 61 cm (24 in.). Collect samples at this depth to get below the surface of the material, since drying and oxidation may have occurred at, or near the surface. Changes in moisture, in particle size, and in other properties continue to occur deeper in the coal and, although not as drastic as near the surface, will cause the method to be biased. The user should review the conditions of the coal (weather conditions, prior transport, settling time, and so forth, see 8.1) so that the interested parties can agree that potential biases are not overly great or that some adjustment in specifications is warranted. Sample increments collected from the surface layer(s) of coal in railroad cars, barges, or stockpiles are classified condition “D” (see Practice D2234/D2234M, Increment Collection Classification). It is a good practice to require that “details of sampling procedure shall be agreed upon in advance by all parties concerned” whenever collection of sample increments falls under condition “D.” This practice offers a sampling procedure that parties may use to meet requirements of Practice D2234/D2234M for condition “D.” The practice does not produce samples that satisfy precision requirements of Practice D2234/D2234M general-purpose sampling, or Practice D2234/D2234M special-purpose sampling.
1.3 The user is cautioned that samples of this type do not satisfy the minimum requirements for probability sampling and as such cannot be used to draw statistical inferences such as precision, standard error, or bias.
1.5 The quantities stated in either acceptable SI units or in inch-pound units are regarded separately as standard. The quantities stated in each system may not be exact equivalents; therefore, each system must be used independently of the other, without combining quantities in any way.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D121 Terminology of Coal and Coke
D2013 Practice for Preparing Coal Samples for Analysis
D2234/D2234M Practice for Collection of a Gross Sample of Coal
D4749 Test Method for Performing the Sieve Analysis of Coal and Designating Coal Size
D4916 Practice for Mechanical Auger Sampling
E105 Practice for Probability Sampling of Materials
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E456 Terminology Relating to Quality and Statistics
ICS Number Code 73.040 (Coals)
UNSPSC Code 15101601(Coal)