Significance and Use
5.1 This test method is used to determine the vulcanization characteristics of (vulcanizable) rubber compounds under selected test conditions of strain and frequency which do not significantly affect the cured dynamic properties. In the same test, this test method also will measure the dynamic properties of the vulcanizate at temperatures significantly below the cure temperature. These lower temperature measurements are necessary in order to more effectively relate to rubber product service conditions.
5.2 This test method may be used for quality control in rubber manufacturing processes and for research and development testing of rubber compounds containing curatives. This test method also may be used for evaluating cure and dynamic property differences resulting from the use of different compounding ingredients.
5.3 For additional information regarding the significance of dynamic testing of vulcanized rubber, the reader may wish to reference Guide D5992.
1.1 This test method covers the use of a rotorless oscillating shear rheometer for measuring after cure dynamic properties at predetermined temperature(s) below the cure temperature.
1.2 Specified cure conditions that approximate a “static cure” also are covered to minimize effects on cured rubber compound dynamic properties. This test method is not intended to replace Test Method D5289.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.4 Warning—Compounds based on silicone or fluoroelastomers may have high levels of thermal contraction or poor adhesion to the dies when cooled after the cure portion of this test method, causing slippage during strain sweeps. If this occurs, the results will not be reliable.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D1349 Practice for Rubber--Standard Temperatures for Testing
D4483 Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
D5289 Test Method for Rubber Property--Vulcanization Using Rotorless Cure Meters
D5992 Guide for Dynamic Testing of Vulcanized Rubber and Rubber-Like Materials Using Vibratory Methods
dynamic properties; loss modulus; rotorless oscillating shear rheometer; storage modulus;
ICS Number Code 83.060 (Rubber)
ASTM International is a member of CrossRef.
Citing ASTM Standards
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