ASTM D6349 - 13

    Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry

    Active Standard ASTM D6349 | Developed by Subcommittee: D05.29

    Book of Standards Volume: 05.06

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    Significance and Use

    5.1 A compositional analysis of coal and coke and their associated combustion residues are often useful in assessing their quality. Knowledge of the elemental composition of the associated residues is also useful in predicting the elemental enrichment/depletion compositional behavior of ashes and slags in comparison to the concentration levels in the parent coal. Utilization of the ash by-products and hazardous potential may also depend on the chemical composition and leachability of the inorganic constituents of the coal ash.

    5.2 The chemical composition of laboratory-prepared ash may not exactly represent the composition of mineral matter in coal or the composition of fly ash and slag resulting from commerical-scale burning of the coal.

    1. Scope

    1.1 This test method covers a procedure for the analysis of the commonly determined major and minor elements in coal, coke, and solid residues from combustion of coal and coke. These residues may be laboratory ash, bottom ash, fly ash, flue gas desulfurization sludge, and other combustion process residues.

    1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D121 Terminology of Coal and Coke

    D346 Practice for Collection and Preparation of Coke Samples for Laboratory Analysis

    D1193 Specification for Reagent Water

    D2013 Practice for Preparing Coal Samples for Analysis

    D3173 Test Method for Moisture in the Analysis Sample of Coal and Coke

    D3174 Test Method for Ash in the Analysis Sample of Coal and Coke from Coal

    D3180 Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases

    D7348 Test Methods for Loss on Ignition (LOI) of Solid Combustion Residues

    D7582 Test Methods for Proximate Analysis of Coal and Coke by Macro Thermogravimetric Analysis

    E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

    ISO Standard

    ISO/IECGuide99:2007 International vocabulary of metrology -- Basic and general concepts and associated terms (VIM)

    ICS Code

    ICS Number Code 75.160.10 (Solid fuels)

    UNSPSC Code

    UNSPSC Code 15101601(Coal); 15101604(Coke)

    DOI: 10.1520/D6349

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