Standards

ASTM D6349 - 09


ASTM D6349 - 09 Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry


Active Standard ASTM D6349 Developed by Subcommittee: D05.29 |Book of Standards Volume: 05.06

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ASTM D6349

Significance and Use

A compositional analysis of coal and coke and their associated combustion residues are often useful in assessing their quality. Knowledge of the elemental composition of the associated residues is also useful in predicting the elemental enrichment/depletion compositional behavior of ashes and slags in comparison to the concentration levels in the parent coal. Utilization of the ash by-products and hazardous potential may also depend on the chemical composition and leachability of the inorganic constituents of the coal ash.

The chemical composition of laboratory-prepared ash may not exactly represent the composition of mineral matter in coal or the composition of fly ash and slag resulting from commerical-scale burning of the coal.

1. Scope

1.1 This test method covers a procedure for the analysis of the commonly determined major and minor elements in coal, coke, and solid residues from combustion of coal and coke. These residues may be laboratory ash, bottom ash, fly ash, flue gas desulfurization sludge, and other combustion process residues.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D346 Practice for Collection and Preparation of Coke Samples for Laboratory Analysis

D1193 Specification for Reagent Water

D2013 Practice for Preparing Coal Samples for Analysis

D3173 Test Method for Moisture in the Analysis Sample of Coal and Coke

D3180 Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases

D5142 Test Methods for Proximate Analysis of the Analysis Sample of Coal and Coke by Instrumental Procedures

E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

ISO Standard

ISO/IECGuide99:2007 International vocabulary of metrology -- Basic and general concepts and associated terms (VIM)



Keywords

coal; coal ash; inductively coupled plasma-atomic emission spectrometry; major and minor element; Coal ash; Coal/coke products--chemical analysis; Composition analysis--coal/coke products; ICP-AES (inductively-coupled plasma atomic emission spectrometry); Major/minor elements;



ICS Code

ICS Number Code 75.160.10 (Solid fuels)



DOI: 10.1520/D6349-09

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