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Significance and Use
5.1 The measurement of particulate matter and collected residue emission rates is an important test method widely used in the practice of air pollution control. Particulate matter measurements after control devices are necessary to determine total emission rates into the atmosphere.
5.2 The collected residue obtained with this test method is also important in characterizing stack emissions. However, the utility of these data is limited unless a chemical analysis of the collected residue is performed.
5.3 These measurements also can be used to calibrate continuous particulate emission monitoring systems by correlating the output of the monitoring instruments with the data obtained by using this test method.
1.1 This test method2 covers a method for the measurement of particulate matter (dust) concentration in emission gases in the concentrations below 20 mg/m3 standard conditions, with special emphasis around 5 mg/m3.
1.3 This test method differs from Test Method D3685/D3685M by requiring the mass measurement of filter blanks, specifying weighing procedures, and requiring monitoring of the flue gas flow variability over the testing period. It requires that the particulate matter collected on the sample filter have a mass at least five times a positive mass difference on the filter blank. High volume sampling techniques or an extension of the sampling time may be employed to satisfy this requirement.
1.4 This test method may be used for calibration of automated monitoring systems (AMS). If the emission gas contains unstable, reactive, or semi-volatile substances, the measurement will depend on the filtration temperature, and in-stack methods may be more applicable than out-stack methods for the calibration of automated monitoring systems.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D1193 Specification for Reagent Water
D1356 Terminology Relating to Sampling and Analysis of Atmospheres
D2986 Practice for Evaluation of Air Assay Media by the Monodisperse DOP (Dioctyl Phthalate) Smoke Test
D3154 Test Method for Average Velocity in a Duct (Pitot Tube Method)
D3631 Test Methods for Measuring Surface Atmospheric Pressure
D3670 Guide for Determination of Precision and Bias of Methods of Committee D22
D3685/D3685M Test Methods for Sampling and Determination of Particulate Matter in Stack Gases
D3796 Practice for Calibration of Type S Pitot Tubes
E1 Specification for ASTM Liquid-in-Glass Thermometers
E2251 Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ISO StandardsISO 10780 Stationary source emissions--Measurement of velocity and volume flow rate of gas stream in ducts ISO 5725 Precision of test methods--Determination of repeatability and reproducibility by inter-laboratory tests ISO 9096 Stationary source emissions--Determination of concentration and mass flow rate of particulate material in gas-carrying ducts. Manual gravimetric method
ICS Number Code 13.040.99 (Other standards related to air quality)
UNSPSC Code 77121500(Air pollution)