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Significance and Use
This test method provides a semiquantitative estimate of the acid number of lubricating oils obtained from laboratory oxidation tests using smaller amounts of sample than Test Methods D 974, D 664, or D 3339
Since this test method is semiquantitative, each laboratory shall develop its own criteria for each oxidation test method for determining when to switch from this semiquantitative test method to a more precise test method for acid number.
1.1 This test method is a semiquantitative micro method intended for monitoring the changes in acidic constituents occurring in lubricating oils during oxidation testing, when the acid number of such oils falls within the range from 0.02 to 1.0 mg of potassium hydroxide per gram of sample. It is applicable to such oils as turbine oils, hydraulic oils, and other circulating oils. Note 1 - This test method is a micro version of Test Method D 974 and it produces results similar to that method.
1.2 This test method is designed for use where sample size is limited. It shall not be used as a replacement for higher precision methods such as Test Methods D 974 or D 664. It shall not be used to monitor oils in-service.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D664 Test Method for Acid Number of Petroleum Products by Potentiometric Titration
D943 Test Method for Oxidation Characteristics of Inhibited Mineral Oils
D974 Test Method for Acid and Base Number by Color-Indicator Titration
D3339 Test Method for Acid Number of Petroleum Products by Semi-Micro Color Indicator Titration
D4871 Guide for Universal Oxidation/Thermal Stability Test Apparatus
ICS Number Code 75.100 (Lubricants, industrial oils and related products)
UNSPSC Code 15120000(Lubricants and oils and greases and anti corrosives)