Significance and Use
This test method is used to determine the quaternary ammonium salts commonly found in fabric softeners. Quaternary ammonium compounds being the active ingredients in fabric softeners requires accurate determination to assess the cost and performance of such compounds.
1. Scope
1.1 This test method describes a potentiometric titration procedure for the determination of quaternary ammonium salts in fabric softeners. This test method is intended for the analysis of known quaternary ammonium salts such as the dialkyl dimethyl quaternary ammonium compound type and the diamidoamine based quaternary ammonium compound type.
1.2 The quaternary ammonium salts conform to the structures shown in Fig.1 and Fig. 2.
1.3 The analytical procedure appears in the following order:
| Section |
| Apparatus | 5 |
| Reagents | 6 |
| Preparation of standard reagents | 7 |
| Standardization of hyamine solution | 9 |
| Safety precautions | 8 |
| Procedure for determination of dialkyl dimethyl quaternaries | 10 |
| Procedure for determination of diamidoamine based quaternaries | 11 |
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 6.4, 6.6, 6.7 and Section 8 for specific warning statements.
2. Referenced Documents (purchase separately)
The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D1193 Specification for Reagent Water
D3049 Test Method for Synthetic Anionic Ingredient by Cationic Titration
Keywords
ICS Code
ICS Number Code 71.060.50 (Salts)
DOI: 10.1520/D5070-90R05
ASTM International is a member of CrossRef.
Citing ASTM Standards
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