Standards

ASTM D4947 - 05


ASTM D4947 - 05 Standard Test Method for Chlordane and Heptachlor Residues in Indoor Air


Active Standard ASTM D4947 Developed by Subcommittee: D22.05 |Book of Standards Volume: 11.07

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ASTM D4947

Significance and Use

This test method is intended to be used primarily for non-occupational exposure monitoring in domiciles, public access buildings and offices.

Chlordane has been used widely as a general insecticide for crops (for example, cotton) and as a termiticide. Heptachlor is a major component of technical chlordane and an insecticide in its own right. Although their use in the United States was discontinued in 1988, residues of the chemicals may remain in indoor air for many years after application.

1. Scope

1.1 This test method covers the sampling and analysis of indoor atmospheres for residues of chlordane and heptachlor.

1.2 This test method is based upon the collection of chlordane and heptachlor from air onto polyurethane foam (PUF) and analysis by gas chromatography coupled with electron capture detection.

1.3 This test method is applicable to concentrations of chlordane varying from 0.1 to 100 g/m3 and heptachlor varying from 0.01 to 80.0 g/m3 with sampling periods to collect at least 0.25 m3 of air. Detection limits will depend upon the conditions of the gas chromatography (GC) and the length of the sampling period.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D1356 Terminology Relating to Sampling and Analysis of Atmospheres
D3686 Practice for Sampling Atmospheres to Collect Organic Compound Vapors (Activated Charcoal Tube Adsorption Method)
D3687 Practice for Analysis of Organic Compound Vapors Collected by the Activated Charcoal Tube Adsorption Method
D4185 Practice for Measurement of Metals in Workplace Atmospheres by Atomic Absorption Spectrophotometry
D4861 Practice for Sampling and Selection of Analytical Techniques for Pesticides and Polychlorinated Biphenyls in Air
E355 Practice for Gas Chromatography Terms and Relationships

EPA Methods

CompendiumofMethodsf

Other Documents

IndoorSamplingGuidel


Index Terms

chlordane; electron capture detection; gas chromatography; heptachlor; indoor air; polyurethane foam;



ICS Code

ICS Number Code 13.040.20 (Ambient atmospheres)



DOI: 10.1520/D4947-05

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