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Significance and Use
5.1 Many petroleum products, and some non-petroleum materials, are used as lubricants, and the correct operation of the equipment depends upon the appropriate viscosity of the liquid being used. In addition, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.
1.1 This test method specifies a procedure for the determination of the kinematic viscosity, ν, of liquid petroleum products, both transparent and opaque, by measuring the time for a volume of liquid to flow under gravity through a calibrated glass capillary viscometer. The dynamic viscosity, η, can be obtained by multiplying the kinematic viscosity, ν, by the density, ρ, of the liquid.
Note 1: For the measurement of the kinematic viscosity and viscosity of bitumens, see also Test Methods and .
Note 2: ISO 3104 corresponds to Test Method – 03.
1.2 The result obtained from this test method is dependent upon the behavior of the sample and is intended for application to liquids for which primarily the shear stress and shear rates are proportional (Newtonian flow behavior). If, however, the viscosity varies significantly with the rate of shear, different results may be obtained from viscometers of different capillary diameters. The procedure and precision values for residual fuel oils, which under some conditions exhibit non-Newtonian behavior, have been included.
1.3 The range of kinematic viscosities covered by this test method is from 0.2 mm2/s to 300 000 mm2/s (see ) at all temperatures (see and ). The precision has only been determined for those materials, kinematic viscosity ranges and temperatures as shown in the footnotes to the precision section.
1.4 The values stated in SI units are to be regarded as standard. The SI unit used in this test method for kinematic viscosity is mm2/s, and the SI unit used in this test method for dynamic viscosity is mPa·s. For user reference, 1 mm2/s = 10-6 m2/s = 1 cSt and 1 mPa·s = 1 cP = 0.001 Pa·s.
1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D446 Specifications and Operating Instructions for Glass Capillary Kinematic Viscometers
D1193 Specification for Reagent Water
D1217 Test Method for Density and Relative Density (Specific Gravity) of Liquids by Bingham Pycnometer
D1480 Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Bingham Pycnometer
D1481 Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer
D2162 Practice for Basic Calibration of Master Viscometers and Viscosity Oil Standards
D2170 Test Method for Kinematic Viscosity of Asphalts (Bitumens)
D2171 Test Method for Viscosity of Asphalts by Vacuum Capillary Viscometer
D6071 Test Method for Low Level Sodium in High Purity Water by Graphite Furnace Atomic Absorption Spectroscopy
D6074 Guide for Characterizing Hydrocarbon Lubricant Base Oils
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
D6300 Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
D6617 Practice for Laboratory Bias Detection Using Single Test Result from Standard Material
D6708 Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material
E1 Specification for ASTM Liquid-in-Glass Thermometers
E77 Test Method for Inspection and Verification of Thermometers
E563 Practice for Preparation and Use of an Ice-Point Bath as a Reference Temperature
E644 Test Methods for Testing Industrial Resistance Thermometers
E1137/E1137M Specification for Industrial Platinum Resistance Thermometers
E1750 Guide for Use of Water Triple Point Cells
E2593 Guide for Accuracy Verification of Industrial Platinum Resistance Thermometers
E2877 Guide for Digital Contact Thermometers
ISO StandardsISO 17025 General Requirements for the Competence of Testing and Calibration Laboratories ISO 3104 Petroleum Products--Transparent and Opaque Liquids--Determination of Kinematic Viscosity and Calculation of Dynamic Viscosity ISO 3105 Glass Capillary Kinematic Viscometers--Specification and Operating Instructions ISO 3696 Water for Analytical Laboratory Use--Specification and Test Methods ISO 5725 Accuracy (trueness and precision) of measurement methods and results. ISO 9000 Quality Management and Quality Assurance Standards--Guidelines for Selection and Use
NIST StandardsNIST GMP 11 Good Measurement Practice for Assignment and Adjustment of Calibration Intervals for Laboratory Standards http://ts.nist.gov/WeightsAndMeasures/upload/GMP_11_Mar_2003.pdf NIST Special Publication 1088 Maintenance and Validation of Liquid-in-Glass Thermometers http://www.nist.gov/pml/pubs/sp1088/index.cfm NIST Special Publication 811 Guide for the Use of the International System of Units (SI) http://www.nist.gov/pml/pubs/sp811/index.cfm NIST Technical Note 1297 Guideline for Evaluating and Expressing the Uncertainty of NIST Measurement Results http://physics.nist.gov/cuu/Uncertainty/bibliography.html
ICS Number Code 17.060 (Measurement of volume, mass, density, viscosity); 75.080 (Petroleum products in general)
UNSPSC Code 15101500(Petroleum and distillates)
ASTM D445-15a, Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity), ASTM International, West Conshohocken, PA, 2015, www.astm.orgBack to Top