ASTM D4266 - 96(2009)e1

    Standard Test Methods for Precoat Capacity of Powdered Ion-Exchange Resins

    Active Standard ASTM D4266 | Developed by Subcommittee: D19.08

    Book of Standards Volume: 11.02


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    Significance and Use

    The salt removal capacity of a powdered resin precoat is limited by the capacity of either the anion-exchange resin or the cation-exchange resin contained in it. Applications include condensate polishing in fossil-fueled electric generating plants, as well as condensate polishing, spent fuel pool water treatment, reactor water treatment, and low-level radioactive liquid waste treatment in nuclear-powered electric generating plants.

    By determining the ion-exchange capacity profile of either a cation exchange resin or an anion-exchange resin (capacity expended per unit of time under specific conditions), it is possible to estimate runlength and remaining capacity when treating a liquid of the same makeup. Although they cannot accurately predict performance during condenser leaks, these test methods are useful for determining operating capacities as measured under the test conditions used.

    These test methods may be used to monitor the performance of either powdered anion-exchange resin or powdered cation-exchange resin. The total capacity of either resin depends primarily upon the number density of ion-exchange sites within the resin. The operating capacity is a function of the total capacity, degree of conversion to the desired ionic form when received, and properties of the resin and the system that affect ion exchange kinetics.

    1. Scope

    1.1 These test methods cover the determination of the operating ion-exchange capacity of both powdered cation-exchange resins (hydrogen form) and powdered anion-exchange resins (hydroxide form). These test methods are intended for use in testing new powdered ion-exchange resins when used for the treatment of water. The following two test methods are included:

    Sections
    Test Method AOperating Capacity, Anion-Exchange
    Resin, Hydroxide Form
    7 to 15
    Test Method BOperating Capacity, Cation-Exchange
    Resin, Hydrogen Form
    16 to 24

    1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.

    1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D1125 Test Methods for Electrical Conductivity and Resistivity of Water

    D1129 Terminology Relating to Water

    D1193 Specification for Reagent Water

    D2687 Practices for Sampling Particulate Ion-Exchange Materials

    D4456 Test Methods for Physical and Chemical Properties of Powdered Ion Exchange Resins

    E200 Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis


    ICS Code

    ICS Number Code 71.100.40 (Surface active agents)

    UNSPSC Code

    UNSPSC Code


    DOI: 10.1520/D4266-96R09E01

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