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Significance and Use
Other standards are used to collect the gross sample: Practice D2234/D2234M allows for one division of the gross sample before crushing. The mass and top size of the gross or divided sample collected by using these guides and practices are usually too large for chemical or physical testing. Practice D2013 provide instructions for reducing and dividing the gross or divided sample, by on-line or off-line processes, or both, to a top size and mass suitable to the performance of testing. Any bias in the gross or divided sample before adherence to this practice will remain in the final sample resulting from use of this practice. Therefore, carefully select the standard to be used to collect the gross sample.
Division and reduction of a sample may occur at more than one location. Most often, the sample is collected, reduced, and divided (one or more times) by use of a mechanical sampling system. The remaining sample may be further divided on-site to facilitate transporting it to the laboratory where further reduction and division likely occurs before analysis.
In places, this practice requires air drying the sample before subsequent reduction. Procedures for air drying and air-dry loss determination are provided in Test Method D3302.
Most often, samples are reduced and divided to an analysis sample. However, some tests may require a sample of different mass or top size. This procedure may be used to provide a sample of any mass and size consist from the gross or divided sample to, and including, the analysis sample.
This practice also specifies how to prepare composite samples, if required.
1.1 This practice covers the reduction and division of gross or divided samples, and the preparation of composite samples, up to and including the individual portions for laboratory analysis.
1.2 Reduction and division procedures are prescribed for coals of the following groups:
1.2.1 Group A includes coals that have been cleaned in all sizes.
1.2.2 Group B includes all other coals. Unknown coals are to be considered under Group B.
1.2.3 Group A allows smaller weight laboratory samples to be retained than Group B. These lower weights may be used for particular coals if they have been shown, by using the procedures of Annex A1.2, to give a sample preparation and analysis variance which is no more than 20 % of the total analysis variance.
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D121 Terminology of Coal and Coke
D2234/D2234M Practice for Collection of a Gross Sample of Coal
D3174 Test Method for Ash in the Analysis Sample of Coal and Coke from Coal
D3302 Test Method for Total Moisture in Coal
D4749 Test Method for Performing the Sieve Analysis of Coal and Designating Coal Size
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E456 Terminology Relating to Quality and Statistics
ICS Number Code 73.040 (Coals)
UNSPSC Code 15101601(Coal)
ASTM D2013 / D2013M-12, Standard Practice for Preparing Coal Samples for Analysis , ASTM International, West Conshohocken, PA, 2012, www.astm.orgBack to Top