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Significance and Use
These test methods are suitable for determining the level of purity and for determining the levels of various impurities. They may be used to establish compliance with specification requirements.
1.1 These test methods cover procedures for the chemical analysis of basic carbonate white lead and basic sulfate white lead.
Note 1—If it is necessary to separate these pigments from others, refer to Practice D 215
1.2 The analytical procedures appear in the following order:
|Preparation of Sample||6|
|Basic Carbonate White Lead:|
|Small Amounts of Iron||7|
|Moisture and Other Volatile Matter||9|
|Carbon Dioxide (Evolution Method)||10|
|Carbon Dioxide and Combined Water (Combustion Method)||11|
|Total Matter Insoluble in Acetic Acid||13|
|Total Matter Insoluble in Acid Ammonium Acetate||14|
|Total Impurities Other Than Moisture||15|
|Basic Sulfate White Lead:|
|Small Amounts of Iron||17|
|Moisture and Other Volatile Matter||19|
|Basic Lead Oxide||22|
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
C25 Test Methods for Chemical Analysis of Limestone, Quicklime, and Hydrated Lime
D185 Test Methods for Coarse Particles in Pigments
D215 Practice for the Chemical Analysis of White Linseed Oil Paints
D280 Test Methods for Hygroscopic Moisture (and Other Matter Volatile Under the Test Conditions) in Pigments
D1193 Specification for Reagent Water
D2371 Test Method for Pigment Content of Solvent-Reducible Paints
D2372 Practice for Separation of Vehicle From Solvent-Reducible Paints
D3280 Test Methods for Analysis of White Zinc Pigments
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
ICS Number Code 87.060.10 (Pigments and extenders)
UNSPSC Code 31211503(Pigment paints)