Standards

ASTM D1157 - 91(2009)


ASTM D1157 - 91(2009) Standard Test Method for Total Inhibitor Content (TBC) of Light Hydrocarbons


Active Standard ASTM D1157 Developed by Subcommittee: D02.D0.04 |Book of Standards Volume: 05.01

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ASTM D1157

Significance and Use

p-tertiary-butylcatechol is commonly added to commercial butadiene in amounts of 50 to 250 mg/kg as an oxidation inhibitor. This test method is suitable for use by both producers and users of butadiene within the limitations described in Section 1.

1. Scope

1.1 This test method covers the determination of total p-tertiary-butylcatechol inhibitor added to polymerization and recycle grades of butadiene or to other C4 hydrocarbon mixtures containing no phenolic material other than catechol or no oxidized phenolic material other than that derived from oxidation of catechol. In general, all phenols and their quinone oxidation products are included in the calculated catechol content. Small amounts of polymer do not interfere. This test method is applicable over the range of TBC from 50 to 500 mg/kg.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D1265 Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method


Keywords

light hydrocarbons; oxidation inhibitor; p-tertiary butylcatechol; photometer; Butadiene (petroleum applications); Inhibitors; Light hydrocarbons; Total inhibitor content (TBC) ;



ICS Code

ICS Number Code 71.080.01 (Organic chemicals in general)



DOI: 10.1520/D1157-91R09

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