Abstract
This test method details the standard and precise procedures for the determination of lead and cadmium extracted by acetic acid from glazed ceramic surfaces. The apparatus needed for this procedure include an atomic absorption spectrometer, lead and cadmium lamps, and glassware of chemical resistant borosilicate glass. The water, detergent wash, and reagents such as acetic acid, lead nitrate solution, hydrochloric acid, and cadmium solution should conform to chemical purity specified. Measurement procedures, precision, and bias are discussed thoroughly.
This abstract is a brief summary of the referenced standard. It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.
1. Scope
1.1 This test method covers the precise determination of lead and cadmium extracted by acetic acid from glazed ceramic surfaces. The procedure of extraction may be expected to accelerate the release of lead from the glaze and to serve, therefore, as a severe test that is unlikely to be matched under the actual conditions of usage of such ceramic ware. This test method is specific for lead and cadmium.
1.2 The values stated in SI (metric) units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Keywords
cadmium; glazed ceramic surfaces; lead; Acetic acid extraction method; Cadmium content--ceramic materials; Cadmium release; Cellulosic fiber insulation; Ceramic whitewares (glazed); Lead content--ceramic materials; Lead release; Spectrophotometry--atomic absorption;
ICS Code
ICS Number Code 81.060.20 (Ceramic products)
DOI: 10.1520/C0738-94R11
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