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Significance and Use
For advanced ceramics, Vickers indenters are used to create indentations whose surface-projected diagonals are measured with optical microscopes. The Vickers indenter creates a square impression from which two surface-projected diagonal lengths are measured. Vickers hardness is calculated from the ratio of the applied load to the area of contact of the four faces of the undeformed indenter. (In contrast, Knoop indenters are also used to measure hardness, but Knoop hardness is calculated from the ratio of the applied load to the projected area on the specimen surface.)
Vickers indentation hardness is one of many properties that is used to characterize advanced ceramics. Attempts have been made to relate Vickers indentation hardness to other hardness scales, but no generally accepted methods are available. Such conversions are limited in scope and should be used with caution, except for special cases where a reliable basis for the conversion has been obtained by comparison tests.
Vickers indentation diagonal lengths are approximately 2.8 times shorter than the long diagonal of Knoop indentations, and the indentation depth is approximately 1.5 times deeper than Knoop indentations made at the same force.
Vickers indentations are influenced less by specimen surface flatness, parallelism, and surface finish than Knoop indentations, but these parameters must be considered nonetheless.
Vickers indentations are much more likely to cause cracks in advanced ceramics than Knoop indentations. The cracks may influence the measured hardness by fundamentally altering the deformation processes that contribute to the formation of an impression, and they may impair or preclude measurement of the diagonal lengths due to excessive damage at the indentation tips or sides.
A full hardness characterization includes measurements over a broad range of indentation forces. Vickers hardness of ceramics usually decreases with increasing indentation size or indentation force. The trend is known as the indentation size effect (ISE). Hardness approaches a plateau constant hardness at sufficiently large indentation size or forces. The test forces or loads that are needed to achieve a constant hardness vary with the ceramic. The test force specified in this standard is intended to be sufficiently large that hardness is either close to or on the plateau, but not so large as to introduce excessive cracking. A comprehensive characterization of the ISE is recommended but is beyond the scope of this test method, which measures hardness at a single, designated force.
1.1 This test method covers the determination of the Vickers indentation hardness of advanced ceramics.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
E4 Practices for Force Verification of Testing Machines
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E384 Test Method for Knoop and Vickers Hardness of Materials
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
European StandardCENENV843-4 Advanced Technical Ceramics, Monolithic Ceramics, Mechanical Properties at Room Temperature, Part 4: Vickers, Knoop and Rockwell Superficial Hardness Available from European Committee for Standardization (CEN), 36 rue de Stassart, B-1050, Brussels, Belgium, http://www.cenorm.be.
Japanese StandardJISR1610 Testing Method for Vickers Hardness of High Performance Ceramics Available from Japanese Standards Organization (JSA), 4-1-24 Akasaka Minato-Ku, Tokyo, 107-8440, Japan, http://www.jsa.or.jp.
ICS Number Code 19.060 (Mechanical testing); 81.060.99 (Other standards related to ceramics)