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SEDL / STP / STP1466-EB
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STP1466
Techniques in Thermal Analysis: Hyphenated Techniques, Thermal Analysis of the Surface, and Fast Rate Analysis
Pan Wei-Ping, Judovits Lawrence
Pages: 132
Published: 2007
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Nine peer-reviewed papers reflect the latest research in thermal analysis, including fast scan calorimetry in both instrument development and techniques. Sections cover: Hyphenated Techniquesseven papers cover the use of thermogravimetric analysis (TGA) with another technique. Topics deal with temperature-modulated differential scanning calorimetry; improved modeling when using hyphenated techniques; a simple calibration method for the quantitative use of mass spectrometry with TGA for a variety of encountered off gases; and much more. Fast Rate Analysiscovers fast scan calorimetry in both instrument development and techniques. Fast heating rates were employed to study epoxy curing and fast rate analysis allowed the separation of the glass transition and cure exotherm. Thermal Analysis of the Surfacediscusses the use of a modified atomic force microscope (AFM), or Micro-Thermal Analysis, that uses the AFM probe as a thermal device.
Table of Contents
An Application of Thermal Analysis to Household Waste
Chen H., Cheng Z., Hack P., Pan W., Zhang Y.
Development and Evaluation of a TG/DTA/Raman System
Bigalow Kern A., Cambron R., Collins W., DuBois C., Redman-Furey N.
The Role of TGA-DTA in the Initial Evaluation of the Solid State Forms for Pharmaceutical New Chemical Entities, Part 1: Evaluation of Pure Forms
Collins W., Dicks M., Godlweski J., Redman-Furey N., Vaughn D.
The Role of TGA-DTA in the Initial Evaluation of the Solid State Forms for Pharmaceutical New Chemical Entities, Part 2: Evaluation of Mixed Forms
Collins W., Dicks M., Godlweski J., Redman-Furey N., Vaughn D.
Use of a TG/DTA/Raman System to Monitor Dehydration and Phase Conversions
Bigalow Kern A., Cambron R., Collins W., Redman-Furey N.
Quantitative Mass Measurements from Mass Spectrometer Trend Data in a TG/MS System
Slough C.
Separation of Overlapping Processes from TGA Data and Verification by EGA
Artiaga R., Cao R., Garcia A., González-Martin B., Mier J., Naya S.
Characterization of Modified Carbon Nanotubes by TG-MS and Pyrolysis-GC/MS
Buthelezi T., Lineberry Q., Pan W.
Characterization Of Epoxy Curing Using High Heating Rate DSC
Bilyeu B., Brostow W., Menard K.
Photo Thermal Micro-Spectroscopy — A New Method for Infared Analysis of Materials
Hammiche A., Pollock H., Reading M., Slough C.
A Thermal Analysis Method for Measuring Polymer Flammability
Lyon R., Stoliarov S., Walters R.
Fast Scan Differential Scanning Calorimetry Distinguishes Melting, Melting-Degradation/Sublimation and Thermal Stability of Drugs
Alexander K., Golinar M., Riga A.
Thermal and Oxidative Properties of Physiologically Relevant Free Fatty Acids by Dielectric Analysis and Differential Scanning Calorimetry
Alexander K., Riga A., Williams K.
Committee: E37
Paper ID: STP1466-EB
DOI: 10.1520/STP1466-EB
ISBN-EB: 978-0-8031-6236-5
ASTM International is a member of CrossRef.
0-8031-5616-2
978-0-8031-5616-6
STP1466-EB
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