Materials Characterization by Dynamic and Modulated Thermal Analytical Techniques

    Riga AT, Judovits L
    Published: 2001

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    STP 1402 examines the latest dynamic and modulated thermal analytical techniques, including new interpretations and applications of Differential Scanning Calorimetry (DSC). The basis of many DSC methods is the modulation of temperature along with varying other parameters. Dynamic methods, including Dynamic Mechanical Analysis (DMA) and Dielectric Thermal Analysis (DETA), are also critiqued with new innovative applications. The mode of modulation, a sinusoidal wave or a saw tooth curve, affords the thermal analyst an opportunity to study a physical or chemical change in greater detail.

    15 peer reviewed papers cover:

    • Temperature Modulated Differential Scanning Calorimetry (TMDSC)

    • Use of TMDSC in Curing and Chemical Reactions

    • Measurement of the Glass Transition and Melting by Modulated and Comparative Techniques

    • General Modulated Techniques

    • Other Modulated Techniques

    • Dynamic Techniques DMA and DETA.

    Table of Contents

    Temperature-Modulated Calorimetry of Polymers with Single and multiple Frequencies to Determine Heat Capacities as Well as Reversible and Irreversible Transition Parameters
    Wunderlich B.

    Measurement of Crystallinity in Polymers Using Modulated Temperature Differential Scanning Calorimetry
    Orliac H., Price D., Reading M.

    Crystallization of Polymers and the Rigid Amorphous Fraction Studied by the Temperature-Modulated Techniques TMDSC and TMDMA
    Merzliakov M., Schick C., Wurm A.

    Evaluation of the Curing Process in a Fiber-Reinforced Epoxy Composite by Temperature-Modulated and Step Scan DSC and DMA
    Bilyeu B., Brostow W., Menard K.

    Effects of TMDSC Variables on the Observed Glass Transitions of Elastomers- a Statistical Analysis
    Burkholder K., Ludwig K., Riga A., Willey J.

    Glass Transformation Studies of Vitreous As2Se3 by Temperature-Modulated DSC
    Kasap S., Tonchev D.

    Comparison Between Modulated Differential Scanning Calorimetry (MDSC) and Dynamic Differential Scanning Calorimetry (DDSC)
    Fuller L., Judovits L.

    Modulated-Temperature Thermomechanical Measurements
    Price D.

    Obtaining Kinetic Parameters Using Modulated Temperature
    Blaine R.

    Analysis of Curing Using Simultaneous Dynamic Mechanical and Dielectric Measurements
    Suwardie J.

    Characterization of Electrorheological Processes By Dielectric Thermal Analysis
    Cahoon J., Pialet J., Riga A.

    Characterization of Organic Surfactants and Dispersants by Frequency-Dependent Dielectric Thermal Analysis and Electrochemistry
    Cahoon J., Lvovich V., Riga A.

    Development of Bismaleimide/Cyanate Ester Copolymers
    Chuang K., Pan W., Sisk B.

    Application of Theory to Prediction and Analysis of Dynamic Mechanical Properties of Polymer Composites
    Goldman A.

    Glass Transition Temperature of Selected Polymers by TMDSC, DMTA and DETA Analyses
    Ceccorulli G., Pizzoli M., Righetti M.

    Author Index

    Subject Index

    Committee: E37

    DOI: 10.1520/STP1402-EB

    ISBN-EB: 978-0-8031-5452-0

    ISBN-13: 978-0-8031-2887-3

    ASTM International is a member of CrossRef.