STP430: The Present Status of Metallography

    Gray, R. J.
    Head, Oak Ridge National Laboratory, Oak Ridge, Tenn

    Pages: 46    Published: Jan 1968


    Abstract

    The metallographer has a prime responsibility as a member of a metallurgical or, in many laboratories, a materials team. In addition to his duties of specimen preparation and assistance in interpretation of microstructures, he must keep abreast of new techniques and developments or develop his own as they are needed.

    The Space Age and particularly the problems of the Nuclear Age have climaxed the obstacles of this field. The daily remote handling of highly radioactive or toxic materials or both, which only a few years ago were textbook curiosities, has removed the “touch” formerly considered an essential part of the operation. Almost all the preparation and investigational steps performed in a conventional laboratory can be carried out by remote operations.

    New techniques in revealing the microstructure in color by staining and anodizing are becoming very popular. Although the colors usually produced have enhanced the art tremendously, the benefit is not confined to beauty. Reaction mechanisms such as corrosion and diffusion as well as variations in crystallographic orientation have been understood more clearly from color interference patterns or basic color changes. This information can be recorded in the laboratory by adopting the present techniques in color photography.

    The development of commercial equipment allied to the objectives of the metallographer has been a big help. The microprobe analyzer permits essential analyses of microscopic areas. Hot stage microscopy equipment allows us to view grain boundary movements and other features formerly confined to the imagination. Quantitative data are obtainable now in a fraction of time formerly required. Along with this development of commercial equipment, there have been “inlab” modifications which show great promise.

    Many challenges remain and new ones can be seen in the near future. One in particular is the uncertainty of availability of well trained or professional metallographers. Current trends in metallurgy and materials science curricula seem to be decreasing the amount of metallographic training. If this trend continues, there will be an even greater requirement for “professional metallographers.”

    Keywords:

    autoradiography, electron microprobes, photomicrography, electron microscopes, etching, field ion microscopes, ion microprobes, laser probes, lineal analysis, metallography, microanalysis, microscopes, phase identification, vacuum deposition, X-rays


    Paper ID: STP41813S

    Committee/Subcommittee: E04.17

    DOI: 10.1520/STP41813S


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