SEDL / STP / STP951-EB / STP19670S



Use of an Inductively Coupled Plasma Emission Spectrometer System in a Separations Process Plant Laboratory

Hiller, JM
Senior chemists, Rockwell Hanford Operations, Richland,WA

Lawry, DH
Senior chemists, Rockwell Hanford Operations, Richland,WA


Pages: 18    Published: Jan 1987


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Source: STP951-EB


Abstract

A commercially available inductively coupled plasma (ICP) emission spectrometry system has been modified and placed into operation for the analysis of radioactive samples in support of a separations process plant. The modifications consisted of building a ported hood around the standard torch box, modifying the gas and electrical connections in and to the torch box, providing an off-gas purification system and providing a shielded drain system. The ICP system, its modifications, support equipment, sample preparation, and two years of working experience are described.


Keywords:
plasma spectroscopy, inductively coupled plasma emission spectrometry, spectrometer, analysis, radioactivity, plutonium, uranium, solvent extraction

Paper ID: STP19670S
Committee/Subcommittee: C26.09
DOI: 10.1520/STP19670S
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