ISSN: 1945-7553
Page Count: 11

Interlaboratory “Pilot Run” Study of Small Heat-Flow-Meter Apparatus for ASTM C 518

Zarr, RR
Mechanical engineer, National Institute of Standards and Technology, Gaithersburg,MD

Lagergren, ES
Mathematical statistician, Nabisco, East Hanover,NJ

(Received 12 October 1998; accepted 27 August 1999)

Abstract

Thermal conductivity measurements of a high-density glass-fiber thermal insulation material near 24°C are presented for the determination of the precision and bias of ASTM Test Method C 518. The measurements have been conducted by 13 laboratories using small (305 by 305-mm) heat-flow-meter apparatus on three specimens of high-density glass-fiber thermal insulation material that were circulated among the laboratories. Test results are analyzed using ASTM Practice E 691 and subsequently compared to measurements of the same specimens conducted in a guardedhot-plate apparatus using ASTM Test Method C 177. The 95% repeatability and reproducibility indexes for precision have been determined to be no worse than 1.1 and 4.0%, respectively. A method for estimating bias is presented.

Keywords:
bias, glass fiber, guarded hot plate, heat flow meter, interlaboratory, precision, repeatability, reproducibility, thermal conductivity, thermal insulation

Paper ID: JTE12163J
DOI: 10.1520/JTE12163J
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