ISSN: 0090-3973
Published Online: 5 December 2005
Page Count: 4

Consolidation of Mechanically Alloyed Titanium Silicide using Polycarbosilane
Srinivasan, MN
Lamar University, TX

Aripaka, SN
Lamar University, TX

(Received 2 April 2004; accepted 3 August 2005)

Abstract

Statistical design of experiments was employed to assess the effect of mechanical alloying variables and the chemical binder, allyl hydridopolycarbosilane (AHPCS), percentage on the crystallite size of mechanically alloyed titanium silicide powder, and the microhardness of samples consolidated by chemical bonding. The results indicate that mechanically alloying the powder with higher milling time, higher milling speed, and lower ball-to-powder ratio, and consolidating with 7.5% AHPCS gives a combination of fine nanocrystalline size in the powder and good microhardness in the compact.

Keywords:
nanostructure, titanium silicide, mechanical alloying, polycarbosilane, crystallite size, microhardness

Paper ID: JTE12615
DOI: 10.1520/JTE12615
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