Volume 3, Issue 6 (June 2006)

    Gravimetric Analysis of the Nonvolatile Residue from an Evaporated Droplet, Using the Quartz Crystal Microbalance/Heat Conduction Calorimeter

    (Received 13 December 2005; accepted 24 March 2006)

    Published Online: 2006

    CODEN: JAIOAD

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    Abstract

    A quartz crystal microbalance/heat conduction calorimeter (QCM/HCC) has been used to determine the nonvolatile residue at the parts-per-million level in 10 µL droplets of methanol and a 45 µL droplet of water. The QCM was used to measure the mass of the nonvolatile residue, and the calorimeter was used to determine the mass of the solvent by the heat required to evaporate the droplet.


    Author Information:

    Smith, AL
    Masscal Corporation, Chatham, MA


    Stock #: JAI13894

    ISSN: 1546-962X

    DOI: 10.1520/JAI13894

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    Author
    Title Gravimetric Analysis of the Nonvolatile Residue from an Evaporated Droplet, Using the Quartz Crystal Microbalance/Heat Conduction Calorimeter
    Symposium Techniques in Thermal Analysis:Hyphenated Techniques, Thermal Analysis of the Surface, and Fast Rate, 2004-05-25
    Committee E37