Volume 38, Issue 1 (January 1993)

    Detection of Trace Explosive Evidence by Ion Mobility Spectrometry

    (Received 4 April 1992; accepted 19 June 1992)

    CODEN: JFSOAD

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    Abstract

    The continuing threat of worldwide terrorism has prompted the need for new and innovative explosives detection systems. As part of an ongoing research effort, the FBI Laboratory has been evaluating new technology and the innovative adaptation of existing technology for use in counterterrorism and counternarcotics investigations. We have been examining the application of ion mobility spectrometry (IMS), for its role in explosives detection.

    The explosives residue is collected on a membrane filter by a special attachment on a household vacuum. Subsequent thermal desorption and analysis requires 5 s. Experimental results have determined the limits of detection for most common explosives to be approximately 200 pg. The vacuum sampling method permits the collection of trace physical evidence transferred to hands or surfaces through contact or post blast residue. The persistence of explosives on hands and transfer to other surfaces has been examined. Post-blast residue of NG was detected on fragments of improvised explosive devices constructed with double-based smokeless powder. Post-blast residue from C-4, Deta Sheet, SEMTEX, and ammonium nitrate explosives have also been detected on items of forensic and evidentiary value.


    Author Information:

    Fetterolf, DD
    Research Chemist, FBI Laboratory, Forensic Science Research Unit, FBI Academy, Quantico, VA

    Clark, TD
    Student, FBI Honors Intern, Department of Chemistry, Southwest Missouri State University, Springfield, MO


    Stock #: JFS13373J

    ISSN: 0022-1198

    DOI: 10.1520/JFS13373J

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    Author
    Title Detection of Trace Explosive Evidence by Ion Mobility Spectrometry
    Symposium , 0000-00-00
    Committee E30