Volume 34, Issue 4 (July 1989)

    The Stereoisomers of 4-Methylaminorex

    (Received 27 August 1988; accepted 17 October 1988)

    CODEN: JFSOAD

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    Abstract

    Physical constants and instrumental data (melting point [mp], thin-layer chromatography [TLC] [Rf], gas chromatography [GC] [Rt], [α]D25, 1H- and 13C-nuclear magnetic resonance [NMR], infrared (IR), 70-eV, electron impact-mass spectroscopy [EI-MS], color, and microcrystalline tests) are reported for the individual stereoisomers, racemates, and corresponding hydrochloride salts of 4-methylaminorex (2-amino-4-methyl-5-phenyl-Δ2-oxazoline, 4,5-dihydro-4-methyl-5-phenyl-2-oxazolamine, McN-822, “U4Euh,” “ICE”). The data allow identification and differentiation of illicit samples of 4-methylaminorex.


    Author Information:

    Sperling, AR
    Forensic chemists, Drug Enforcement Administration, Special Testing and Research Laboratories, McLean, VA

    Cooper, DA
    Forensic chemists, Drug Enforcement Administration, Special Testing and Research Laboratories, McLean, VA

    Klein, RFX
    Forensic chemists, Drug Enforcement Administration, Special Testing and Research Laboratories, McLean, VA

    Kram, TC
    Forensic chemists, Drug Enforcement Administration, Special Testing and Research Laboratories, McLean, VA


    Stock #: JFS12723J

    ISSN: 0022-1198

    DOI: 10.1520/JFS12723J

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    Author
    Title The Stereoisomers of 4-Methylaminorex
    Symposium , 0000-00-00
    Committee E30