ASTM WK46273

    New Test Method for Determination Perfluorinated Compounds in Water, Sludge, Influent, Effluent, Wastewater by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS).

    (What is a Work Item?)

    Developed by Subcommittee: D19.06 | Committee D19 | Contact Staff Manager



    WK46273

    1. Scope

    This procedure covers the quick, cheap, reliable and effective method for analysis of selected perfluorinated compounds (PFCs) (perfluoroalkyl carboxylates, perfluoroalkyl sulfonates, and fluorotelomer acids) in a water matrix by filtration followed by liquid chromatography/tandem mass spectrometry analysis. The samples are prepared in 50% methanol (for sludge samples- under basic condition at pH ~ 9-10 by adding ammonium hydroxide), filtered, and then acidified with acetic acid (pH ~ 3-4) and analyzed by liquid chromatography/tandem mass spectrometry.

    Standard for the analysis of PFCs that can be used to monitor waters. Very fast sample preparation and analysis.


    Keywords

    Mass spectrometry, Fluorinated chemicals, survey analysis. Quick easy sample preparation and analysis.

    The title and scope are in draft form and are under development within this ASTM Committee.

    Citing ASTM Standards
    Back to Top
    Work Item Status

    Date Initiated:
    05-27-2014

    Technical Contact:
    Lawrence Zintek

    Item:
    003

    Ballot:
    D19.06 (14-02)

    Status:
    In Balloting