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ASTM WK29923

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Work Item: ASTM WK29923 - Revision of D4927 - 10 Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy


Active Standard: D4927 - 10

Developed by Subcommittee: D02.03 | Committee D02 Home | Contact Staff Manager



1. Rationale

The current 6.3 identifies a limited number of suitable film materials which can be used to cover disposable x-ray cells. The suitable films listed include film materials which were available at the time the method was developed. Newer film materials have become available which are more resistant to leakage and provide statistically comparable results for D4927 (see supporting Research Report). The proposed revision is being made to update 6.3 in order to allow newer x-ray cell window film materials to be used when doing a D4927 analyses with supporting data.


Keywords

additives; barium; calcium; lubricating oil; phosphorous; sulfur; wavelength-dispersive; X-ray fluorescence; zinc; Additives--lubricating oils; Barium content--petroleum products; Calcium content--petroleum products; Chemical analysis--petroleum products; Elemental analysis; Fuel sulfur; Lubricants (fluid); Lubricating oils; Petroleum products; Petroleum products (liquid); Phosphorus content--petroleum products; Spectroscopy--X-ray fluorescence (XRF); Wavelength dispersive X-ray fluorescence (WDXRF); XRF (X-ray fluorescence)--petroleum products; Zinc content--petroleum products; Additives--lubricating oils; Barium content--petroleum products; Calcium content--petroleum products; Chemical analysis--petroleum products; Elemental analysis; Fuel sulfur; Lubricants (fluid); Lubricating oils; Petroleum products; Petroleum products (liquid); Phosphorus content--petroleum products; Spectroscopy--X-ray fluorescence (XRF); Wavelength dispersive X-ray fluorescence (WDXRF); XRF (X-ray fluorescence)--petroleum products; Zinc content--petroleum products;

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Work Item Status:
Date Initiated:08-09-2010
Technical Contact: Rey Montemayor

Status: Draft Under Development

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