Standard Withdrawn, No replacement   Last Updated: Dec 31, 2010 Track Document
ASTM F111-96(2002)

Standard Practice for Determining Barium Yield, Getter Gas Content, and Getter Sorption Capacity for Barium Flash Getters (Withdrawn 2008)

Standard Practice for Determining Barium Yield, Getter Gas Content, and Getter Sorption Capacity for Barium Flash Getters (Withdrawn 2008) F0111-96R02 ASTM|F0111-96R02|en-US Standard Practice for Determining Barium Yield, Getter Gas Content, and Getter Sorption Capacity for Barium Flash Getters (Withdrawn 2008) Standard new BOS Vol. 10.04 Committee F01
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Scope

1.1 This practice describes techniques for the determination of evaporated barium yield, getter gas content, and getter carbon monoxide sorption capacity for barium flash getters used in electron devices. Test conditions are chosen to approximate use conditions.

1.2 Auxiliary procedures for cleaning, for determining vacuum system leak-up rates, for flashing getters, and for determining barium content in both getter fill and films are also given.

1.3 The various tests described are destructive in nature. In general the tests are semiquantitative but they can be expected to yield comparative information on a single-laboratory basis to the precision indicated. No information relative to multilaboratory reproducibility is available.

1.4 List of Methods Described

MethodSection
Barium Content, Determination of,9
Acid-Base Titration Method9.6
Complexation (Titration) Method9.7
Gravimetric Method9.4
Photometric Method9.5
Weight Difference Method9.8
Barium Yield, Determination of,10
Carbon Monoxide Sorption Characteristics, Determination of12
Cleaning Procedures6
Getter Mount6.3
Getter Test Bulb6.4
Flashing Procedures8
Gas Content, Determination of for Doped Getters:11
Hydrogen11.7
Nitrogen for Undoped Getters:11.8
Preflash Gas Content11.5
Total Gas Content11.4
Leak-Up Rates, Determination of7

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of whoever uses this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 4.

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