Significance and Use
The test methods in this standard are designed to show whether a given material meets the specifications prescribed in Specification C 967.
Because of the variability of matrices of uranium-ore concentrate and the lack of suitable reference or calibration materials, the precision and bias of these test methods should be established by each individual laboratory that will use them. The precision and bias statements given for each test method are those reported by various laboratories and can be used as a guideline.
Instrumental test methods such as X-ray fluorescence and emission spectroscopy can be used for the determination of some impurities where such equipment is available.
1. Scope
1.1 These test methods cover procedures for the chemical and atomic absorption analysis of uranium-ore concentrates to determine compliance with the requirements prescribed in Specification C 967.
1.2 The analytical procedures appear in the following order:
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. A specific precautionary statement is given in Section 7.
2. Referenced Documents
C1110 Practice for Sample Preparation for X-Ray Emission Spectrometric Analysis of Uranium in Ores Using the Glass Fusion or Pressed Powder Method
C1219 Test Methods for Arsenic in Uranium Hexafluoride
C1254 Test Method for Uranium in Mineral Acids by X-Ray Fluoresence
C1267 Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followeed by Chromium (IV) Titration in the Presence of Vanadium
C1287 Test Method for Determination of Impurities in Nuclear Grade Uranium Compounds by Inductively Coupled Plasma Mass Spectrometry
C1347 Practice for Preparation and Dissolution of Uranum Materials for Analysis
C761 Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium Hexafluoride
C859 Terminology Relating to Nuclear Materials
C967 Specification for Uranium Ore Concentrate
D1193 Specification for Reagent Water
E60 Practice for Photometric and Spectrophotometric Methods for Chemical Analysis of Metals
Index Terms
concentrates; uranium ore; ICS Number Code 27.120.30
DOI: 10.1520/C1022-05

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