Standard Historical Last Updated: May 15, 2013 Track Document
ASTM E2554-07

Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method in a Single Laboratory Using a Control Sample Program

Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method in a Single Laboratory Using a Control Sample Program E2554-07 ASTM|E2554-07|en-US Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method in a Single Laboratory Using a Control Sample Program Standard new BOS Vol. 14.01 Committee E11
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Significance and Use

Laboratories accredited under ISO 17025 are required to present uncertainty estimates for their test results. This practice provides procedures that use test results to develop uncertainty estimates for an individual laboratory.

Generally, these test results will be from a single sample of stable and homogeneous material known as a control or check sample.

The true value of the characteristic(s) of the control sample being measured will ordinarily be unknown. However, this methodology may also be used if the control sample is a reference material, in which case the test method bias may also be estimated and incorporated into the uncertainty estimate. Many test methods do not have true reference materials available to provide traceable chains of uncertainty estimation.

This practice also allows for ongoing monitoring of the laboratory uncertainty. As estimates of the level of uncertainty change, possibly as contributions to uncertainty are identified and minimized, revision to the laboratory uncertainty will be possible.

Scope

1.1 This practice describes techniques for a laboratory to estimate the uncertainty of a test result using data from test results on a control sample.

1.2 Uncertainty as defined by this practice applies to the capabilities of a single laboratory. Any estimate of uncertainty determined through the use of this practice applies only to the individual laboratory for which the data are presented.

1.3 The laboratory uses a well defined and established test method in determining a series of test results. The uncertainty estimated using this practice only applies when the same test method is followed. The uncertainty only applies for the material types represented by the control samples, and multiple control samples may be needed, especially if the method has different precision for different sample types or response levels.

1.4 The uncertainty estimate determined by this practice represents the intermediate precision of test results. This estimate seeks to quantify the total variation expected within a single laboratory using a single established test method while incorporating as many known sources of variation as possible.

1.5 This practice does not establish error estimates (error budget) attributed to individual factors that could influence uncertainty.

1.6 This practice describes the use of control charts to evaluate the data obtained and presents a special type of control chart to monitor the estimate of uncertainty.

1.7 The system of units for this Standard is not specified. Dimensional quantities in the Standard are presented only as illustrations of calculation methods. The examples are not binding on products or test methods treated.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Details
Book of Standards Volume: 14.01
Developed by Subcommittee: E11.20
Pages: 7
DOI: 10.1520/E2554-07
ICS Code: 03.120.10; 19.020